ACID ESTERIFICATION
#1
ACID ESTERIFICATION
I got ahold of about 100 gallons of oil that is titrating very high and when i try and do the transesterification it just turns into glop. I have read a little about putting sulfuric acid into the oil with methanol and mixing it to lower the titration numbers. Anyone using this method?
#4
#5
Could also try and find a different source of oil and mix the two together to get lower titration. Have done this too...
#6
#7
I got ahold of about 100 gallons of oil that is titrating very high and when i try and do the transesterification it just turns into glop. I have read a little about putting sulfuric acid into the oil with methanol and mixing it to lower the titration numbers. Anyone using this method?
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#9
I got it from a local conveinence store and i dont know what type of oil it is so i guess im a little lost. Im making 1 liter batches just to test with and they have all come out as glop using this method
1L oil
200ml methanol
+5 whatever i titrate NAOH
I have also heated each batch to about 300F on my stove to get the water out. Any other suggestions on getting water out? The oil looks milky before i heat it and then after its heated and cooled you can see thru it. Any suggestions appreciated.
1L oil
200ml methanol
+5 whatever i titrate NAOH
I have also heated each batch to about 300F on my stove to get the water out. Any other suggestions on getting water out? The oil looks milky before i heat it and then after its heated and cooled you can see thru it. Any suggestions appreciated.
#10
Could be several thing i guess. One is it could be a synthetic veg oil. It also sounds like it may be partally hydronated oil to. There is a place were i get there oil and they use a creamy butter type stuff. I mix it in with my other oil. Also you could try KoH. It is more tolerant of high titrating oil and titration mistakes.
#11
#13
Filtering doesn't remove water, but it does help with titration due to removing the bigger chunks. I don't filter that small going into the processor though, through screen first then a paint strainer (100 micron?) See my gallery. Filter into 55 gallon plastic drum, with output into reactor at the 20 gallon level. Crap that makes it through the filter settles to the bottom of the barrel and is drained off. With Turner and Fab on using KOH.
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